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The recovery of hafnium free zirconium x jras greater tlian 96 per cent The source material for zirconium was the reaction product of caustic soda and zircon sand. The reaction product was leached with water to remove the water soluble silicates and then was dissolved in sulfuric acid. The zirconium was precipitated as zirconium Itydroxide.
A process is provided for separating zirconium and hafnium tetrachlorides by the direct distillation from their solution in an eutectic mixture of sodium and potassium chlorides. Hafnium tetrachloride and zirconium tetrachloride are provided in adequate purity for direct introduction into reduction units for the production of the respective metals by virtue of controlled ratios of the salt.
Australia now has the biggest share of zirconium reserves as a single country. Zirconium mine production In 2013, global zirconium production totaled 1.44 million tonnes，registering a 1.4 year on year drop. Nearly half of the world’s zirconium (42 ) was produced in Australia, followed by 25 in South Africa and 10 in China.
The recently developed new process based on molten salt metal equilibrium for Zr–Hf separation shows a great potential for industrial application, which is compact for nuclear grade zirconium production starting from crude ore. In the present paper, the available separation technologies are compared.