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Liquid Nitrogen For Sulphur Grinding

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Liquid Nitrogen For Sulphur Grinding

For samples grinding at high (70 C) or low temperature (−70 C with extra low temperature freezer for powder), they were equilibrated for 20 min before grinding. For grinding in liquid nitrogen (for EPR analysis), the Dewar flask, full of liquid nitrogen, was put into a glove box. The scintillation vials were immersed in liquid nitrogen.

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